Determination of the phenol compounds in concrete using GC-MS

Organic contaminants from building materials negatively affected people's health. This study presents the validation of the analytical method, developed for the simultaneous identification and quantification of 9 phenolic compounds: phenol, 2-chloro phenol, 2,4-dimethyl phenol, 2,4-dichlorophen...

Full description

Saved in:
Bibliographic Details
Main Authors: Savić Branislava
Mihajlović Ivana
Brdarić Tanja
Krivokapić Nevena
Seović Mina
Nikolić Željka
Corporate Author: International Symposium on Analytical and Environmental Problems (23.) (2017) (Szeged)
Format: Book part
Published: 2017
Series:Proceedings of the International Symposium on Analytical and Environmental Problems 23
Kulcsszavak:Fenolok, Beton, Kémia
Online Access:http://acta.bibl.u-szeged.hu/56214
Description
Summary:Organic contaminants from building materials negatively affected people's health. This study presents the validation of the analytical method, developed for the simultaneous identification and quantification of 9 phenolic compounds: phenol, 2-chloro phenol, 2,4-dimethyl phenol, 2,4-dichlorophenol, 2,6-dichlorophenol, 4-chloro-3-methyl phenol, 2,4,6-trichlorophenol, 2,3,4,6-tetrahydrophenol, pentachlorophenol in solid-solid concrete by gas chromatographic method with mass spectrometric detection (GC-MS). By comparing the MS spectra of the test compounds with MS spectra of analytical standards, reliable identification was achieved. The method can be applied in a given range (from 0.01 to 7.5 mg/kg) with the appropriate parameters precision, accuracy, repeatability and linearity. The developed method could be used for the quality control testing of phenols in concrete during the construction of new buildings and the old residences.
Physical Description:313-316
ISBN:978-963-306-563-1