Synthesis and characterization of CdS nanocrystals in Maleic anhydride–Octene-1–Vinylbutyl Ether terpolymer matrix

Abstract A Maleic anhydride–Octene-1–Vinylbutyl Ether terpolymer was synthesized via the radical terpolymerization method in order to prepare a new matrix for CdS nanocrystal synthesis. CdS nanocrystals were synthesized through the reaction of thiourea with cadmium chloride. The synthesized terpolym...

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Elmentve itt :
Bibliográfiai részletek
Szerzők: Akperov Oktay H.
Muradov Mustafa B.
Malikov Elvin Y.
Akperov Elchin O.
Mammadova Rasmiyya E.
Eyvazova Goncha M.
Kukovecz Ákos
Kónya Zoltán
Dokumentumtípus: Cikk
Megjelent: 2016
Sorozat:PHYSICA E-LOW-DIMENSIONAL SYSTEMS & NANOSTRUCTURES 81
doi:10.1016/j.physe.2016.03.012

mtmt:3174232
Online Access:http://publicatio.bibl.u-szeged.hu/11051
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100 1 |a Akperov Oktay H. 
245 1 0 |a Synthesis and characterization of CdS nanocrystals in Maleic anhydride–Octene-1–Vinylbutyl Ether terpolymer matrix  |h [elektronikus dokumentum] /  |c  Akperov Oktay H. 
260 |c 2016 
300 |a 150-155 
490 0 |a PHYSICA E-LOW-DIMENSIONAL SYSTEMS & NANOSTRUCTURES  |v 81 
520 3 |a Abstract A Maleic anhydride–Octene-1–Vinylbutyl Ether terpolymer was synthesized via the radical terpolymerization method in order to prepare a new matrix for CdS nanocrystal synthesis. CdS nanocrystals were synthesized through the reaction of thiourea with cadmium chloride. The synthesized terpolymer/CdS nanocrystal composites were characterized by several methods. Energy Dispersive X-ray analysis, Raman spectroscopy and powder X-ray diffraction methods. The room temperature UV–visible absorption spectra show a shift of the absorption edge towards higher energies. The band gap of the CdS nanocomposite is bigger than that of bulk CdS. Raman spectrum exhibits characteristic peaks of CdS. Images of the nanocomposite obtained with Atomic Force Microscopy and Transmission Electron Microscopy are the evidences of CdS nanocrystal formation in the terpolymer. Thermal investigation shows that the nanocomposite is more thermostable than the terpolymer which could be useful for application in thermo aggressive medium. 
700 0 1 |a Muradov Mustafa B.  |e aut 
700 0 1 |a Malikov Elvin Y.  |e aut 
700 0 1 |a Akperov Elchin O.  |e aut 
700 0 1 |a Mammadova Rasmiyya E.  |e aut 
700 0 1 |a Eyvazova Goncha M.  |e aut 
700 0 1 |a Kukovecz Ákos  |e aut 
700 0 1 |a Kónya Zoltán  |e aut 
856 4 0 |u http://publicatio.bibl.u-szeged.hu/11051/1/1_s2.0_S1386947716300765_main_u.pdf  |z Dokumentum-elérés