Amine functionalized KIT-6 for CO2 adsorption at different temperatures

In this paper, pure KIT-6 was synthesized and functionalized with 3-aminopropyl triethoxysilane (APTES) by grafting in aqueous solvent at 80°C. The as-prepared composites were characterized by X-ray diffraction at low angles, FT-IR spectroscopy, TGA-DTA coupled with mass-spectrometry, SEM and N2 phy...

Teljes leírás

Elmentve itt :
Bibliográfiai részletek
Szerzők: Suba Mariana
Verdes Orsina
Popa Alexandru
Borcanescu Silvana
Testületi szerző: International Symposium on Analytical and Environmental Problems (25.) (2019) (Szeged)
Dokumentumtípus: Könyv része
Megjelent: 2019
Sorozat:Proceedings of the International Symposium on Analytical and Environmental Problems
Kulcsszavak:Adszorpció, Kémia
Online Access:http://acta.bibl.u-szeged.hu/64843
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520 3 |a In this paper, pure KIT-6 was synthesized and functionalized with 3-aminopropyl triethoxysilane (APTES) by grafting in aqueous solvent at 80°C. The as-prepared composites were characterized by X-ray diffraction at low angles, FT-IR spectroscopy, TGA-DTA coupled with mass-spectrometry, SEM and N2 physisorption techniques followed by testing for CO2 adsorption at different temperatures. The CO2 adsorption/desorption performance was investigated by TGA-DTA coupled with mass-spectrometry using TPD method. The results showed that the CO2 adsorption capacity decreases with increasing temperature from 40 to 70 °C. 
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